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Influence of milling time during the mechanical alloying process on the properties of Fe-3Si-0.75P alloy

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Influence of milling time during the mechanical alloying process on the properties of Fe-3Si-0.75P alloy

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Título Influence of milling time during the mechanical alloying process on the properties of Fe-3Si-0.75P alloy
Autor Pelegrini, Leandro
Bittencourt, Sérgio Deitos
Pauletti, Philippe
Verney, Jose Carlos Krause de
Dias, Moisés de Mattos
Schaeffer, Lirio
Abstract In this study the soft magnetic alloy Fe-3Si-0.75P (wt%) was obtained by mechanical alloying through powder metallurgy. The processing included the formulation of metallic powder, wet milling for 1 h, 3 h, 6h and 9 h, in an attritor mill using alcohol P.A. as a lubricant. Cold compaction was then performed in a floating die under 600 MPa pressure and, finally the ring-shaped test specimens were sintered at 1150 °C for 1h. The electrical, physical and magnetic properties were then analyzed using the following assays: Laser granulometry, density, metallography, hysteresis curve and AC permeability, resistivity and XRD. The results showed a strong influence of milling time on magnetic properties of the alloy. There was a decrease in grain size with the milling time, which is likely the cause of increased in magnetic properties.
Contido em Materials research : ibero-american journal of materials. São Carlos, SP. Vol. 18, n. 5 (Sept./Oct. 2015), p. 1070-1076
Assunto Ligas de ferro-silício
Materiais magneticos
Metalurgia do pó
[en] Mechanical alloying
[en] Powder metallurgy
[en] Soft magnetic materials
Origem Nacional
Tipo Artigo de periódico
URI http://hdl.handle.net/10183/132785
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